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Beilstein J. Org. Chem. 2013, 9, 1517–1525, doi:10.3762/bjoc.9.173
Graphical Abstract
Scheme 1: Methods of synthesis of 3-nitro-1-phenyl-1H-pyrazole (3a) described in the literature.
Figure 1: X-ray structure of 3-nitro-1-[4-(trifluoromethoxy)phenyl]-3-nitro-1H-pyrazole (3k) with 60% probabi...
Scheme 2: Cross coupling of 3-nitro-1H-pyrazole (1a) with phenylboronic acid (2a).
Scheme 3: Cross coupling of 1a with arylboronic acids 2a–n.
Scheme 4: Cross coupling of C-nitro-NH-azoles 1a–d with phenylboronic acid (2a).